LXX Gen 42:22

ἀποκριθεὶς δὲ Ῥουβὴν εἶπεν αὐτοῖς ὐκ ἐλάλησα ὑμῖν λέγων Μὴ ἀδικήσητε τὸ παιδάριον ; καὶ οὐκ εἰσηκούσατέ μου· καὶ ἰδοὺ τὸ αἷμα αὐτοῦ ἐκζητεῖται.

And Reuben responded, “Didn’t I tell you not to sin against the boy? But you would not listen. Now we must account for his blood!”